HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetyl chloride → 4-(2-Methoxy-benzylidene)-morpholin-4-ium chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | Morpholine | HCID 8083 | — |
| Edukt | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Produkt | 4-(2-Methoxy-benzylidene)-morpholin-4-ium chloride | HCID 15551911 | — |
Reaktionsschritte
The reaction of 18.8 ml (0.216 mol) morpholine and 12.4 g (0.09 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 5.3 ml (0.110 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.61 g (corresponding to 38% of the yield calculated by theory) 4-(2-methoxy-benzylidene)-morpholin-4-ium chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07091220B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-12e6a2521fd3401ea452a00a23616dfb |
| Quellennotiz | uspto-grants-2006_08 |