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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 9027Erstellt: 24. Oktober 2026

Dimethylamine → 2-Methoxy-benzylidene-dimethyl-ammonium chloride

https://huagongshe.com/de/reaction/9027

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDimethylamineHCID 674—
EduktAcetyl chlorideHCID 6367—
Edukt2-MethoxybenzaldehydeHCID 8658—
Produkt2-Methoxy-benzylidene-dimethyl-ammonium chlorideHCID 21985303—

Reaktionsschritte

The reaction of 17.0 ml (0.135 mol) dimethylamine solution and 6.8 g ml (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 3.0 ml (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 4.8 g (corresponding to 48% of the yield calculated by theory) 2-methoxy-benzylidene-dimethyl-ammonium chloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07091220B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-6fc688613ae646f2a32ab26807d5074f
Quellennotizuspto-grants-2006_08