HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethylamine → N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethylamine | HCID 8021 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | p-Menthane-3-carboxylic acid | HCID 97896 | — |
| Edukt | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
| Produkt | N,N-Diethyl-2-isopropyl-5-methylcyclohexanecarboxamide | HCID 93591 | — |
Reaktionsschritte
Following the procedure of Example 5, p-menthane-3-carboxylic acid (1.84 g.) was reacted with thionyl chloride and the p-menth-3-oyl chloride then reacted with diethylamine (0.74 g.) in the presence of sodium hydroxide (0.4 g.). The product N,N-diethyl-p-menthane-3-carboxamide was recovered.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04226988 |
| Quelldatensatz | uspto-grants-1980_10 |
| ORD ID | ord-55af27376aad4328a0e398514800ad87 |
| Quellennotiz | uspto-grants-1980_10 |