Ethanol → 2-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine

Beteiligte Stoffe

Reaktionsschritte

A solution of sodium (0.46 g.) in ethanol (50 ml.) was added with stirring and waterbath cooling (25° C.) to a solution of the dichlorotriazine (3.86 g.) from (a) in ethanol (50 ml.). Following the addition the solution was poured into ice water (250 ml.) and the product collected, dried and crystallised from petroleum as needles (2.5 g.) having a melting point of 124° C.

Herkunft & Nachweise