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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 903887Erstellt: 24. Oktober 2026

2-Oxobutanoic Acid → Thiazolidinecarboxylic acid, 2-ethyl-

https://huagongshe.com/de/reaction/903887

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-Oxobutanoic AcidHCID 58—
EduktTriethylamineHCID 8471—
EduktCysteamine HydrochlorideHCID 9082—
LösungsmittelEthanolHCID 702—
ProduktThiazolidinecarboxylic acid, 2-ethyl-HCID 19846265,8%

Reaktionsschritte

11.4 g of cysteamine hydrochloride and 10.1 g of triethylamine were dissolved in 100 ml of ethanol, to which was added 10.2 g of 2-keto-butyric acid. The mixture was refluxed for 30 minutes, cooled and filtered thereby giving 10.6 g (yield 65.7%) of 2-ethyl-thiazolidine-2-carboxylic acid with a melting point of 235°-238° C. (decomposed).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04229461
Quelldatensatzuspto-grants-1980_10
ORD IDord-6417e3b5d0cb4c31933f5935b2dc8ca2
Quellennotizuspto-grants-1980_10