Butyl Formate → Dibutyl Oxalate

HRID 904933

Reaktionsgleichung

Reaktionsgleichung von HRID 904933
[CH:1]([O:3][CH2:4][CH2:5][CH2:6][CH3:7])=[O:2]>C(O)CCC>[C:1]([O:3][CH2:4][CH2:5][CH2:6][CH3:7])(=[O:2])[C:1]([O:3][CH2:4][CH2:5][CH2:6][CH3:7])=[O:2]

Komponenten

3

Edukt 1

HCID 11614Butyl Formate

Produkt 1

HCID 16306Dibutyl Oxalate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 2631-ButanolLösungsmittel

Versuchsvorschrift

Experiment was run in the same manner as in Example 4 except that the catalyst was replaced by 1.0 wt.% palladium-on-silicon-carbide. As the result, it was found that n-butyl formate was produced in a space time yield of 202 g./l.-catalyst.hr and small amounts of di-n-butyl oxalate and n-butanol were by-produced.

Aufarbeitung

  1. customwas produced in a space time yield of 202 g

Quellen und Nachweise

ORD-Eintrag
ord-57f0fcd15f7c4a6a815b1edb34f42b7d
Quelldatensatz
uspto-grants-1983_12
Patentnummer
US04420633

Verknüpfte Notizen

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