Dimethylamine → [(2,3-Dimethoxy-phenyl)-(4-nitro-1H-indol-3-yl)-methyl]-dimethylamine

HRID 9054

Reaktionsgleichung

Reaktionsgleichung von HRID 9054
[N+:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:5]=1[CH:6]=[CH:7][NH:8]2)([O-:3])=[O:2].[Cl-].[CH3:14][O:15][C:16]1[C:25]([O:26][CH3:27])=[CH:24][CH:23]=[CH:22][C:17]=1[CH:18]=[N+:19]([CH3:21])[CH3:20].COC1C(OC)=CC=CC=1C=O.CNC>>[CH3:14][O:15][C:16]1[C:25]([O:26][CH3:27])=[CH:24][CH:23]=[CH:22][C:17]=1[CH:18]([N:19]([CH3:21])[CH3:20])[C:6]1[C:5]2[C:9](=[CH:10][CH:11]=[CH:12][C:4]=2[N+:1]([O-:3])=[O:2])[NH:8][CH:7]=1

Komponenten

5

Edukt 4

HCID 674DimethylamineHCID 665812,3-DimethoxybenzaldehydeHCID 1457664-Nitro-1H-indoleHCID 21985319(2,3-Dimethoxy-benzylidene)-dimethylammonium chloride

Produkt 1

HCID 21985349[(2,3-Dimethoxy-phenyl)-(4-nitro-1H-indol-3-yl)-methyl]-dimethylamine

Versuchsvorschrift

The preparation was carried out in accordance with general synthesis instructions 4 from 4-nitro-1H-indole and (2,3-dimethoxy-benzylidene)-dimethylammonium chloride, which had been prepared in accordance with example 44 from 2,3-dimethoxy-benzaldehyde and dimethylamine.

Quellen und Nachweise

ORD-Eintrag
ord-587b5a90563d478ba07650bd7b8c540a
Quelldatensatz
uspto-grants-2006_08
Patentnummer
US07091220B2

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