Benzylamine → HCID 67386187, Verbindung

Reaktionsgleichung

[C:1]([O:5][C:6]([N:8]1[CH2:14][CH2:13][C:12](=O)[CH:11]([CH3:16])[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:17]([NH2:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:1]([O:5][C:6]([N:8]1[CH2:9][CH2:10][CH:11]([CH3:16])[CH:12]([NH:24][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH2:13][CH2:14]1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Komponenten

Edukt 2

HCID 7504Benzylamine

HCID 20594186Tert-butyl 4-methyl-5-oxoazepane-1-carboxylate

Produkt 1

HCID 67386187HCID 67386187, Verbindung

Versuchsvorschrift

Racemic 4-benzylamino-5-methyl-azepane-1-carboxylic acid tert-butyl ester was prepared in the same manner from racemic 4-methyl-5-oxo-azepane-1-carboxylic acid tert-butyl ester. In this instance, benzylamine was used instead of (R)-1-phenylethylamine.

Quellen und Nachweise

ORD-Eintrag: ord-9d2e21e7b3c4449895c813c2d49e12c6
Quelldatensatz: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08012974B2

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