3-[(4,5-Dimethyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester → 3-[(4,5-Dimethyl-furan-2-ylmethyl)-amino]-phthalic acid

HRID 906803

Reaktionsgleichung

Reaktionsgleichung von HRID 906803
C[O:2][C:3](=[O:23])[C:4]1[C:5](=[C:10]([NH:14][CH2:15][C:16]2[O:17][C:18]([CH3:22])=[C:19]([CH3:21])[CH:20]=2)[CH:11]=[CH:12][CH:13]=1)[C:6]([O:8]C)=[O:7].COCCNC1C=CC=C(C(O)=O)C=1C(O)=O>>[CH3:21][C:19]1[CH:20]=[C:16]([CH2:15][NH:14][C:10]2[CH:11]=[CH:12][CH:13]=[C:4]([C:3]([OH:23])=[O:2])[C:5]=2[C:6]([OH:8])=[O:7])[O:17][C:18]=1[CH3:22]

Komponenten

3

Edukt 2

HCID 210401303-[(4,5-Dimethyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl esterHCID 219885193-(2-Methoxy-ethylamino)-phthalic acid

Produkt 1

HCID 219885163-[(4,5-Dimethyl-furan-2-ylmethyl)-amino]-phthalic acid

Versuchsvorschrift

3-[(4,5-Dimethyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester (0.95 g, 3 mmol) was treated in the same manner as described above for the synthesis of 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.

Aufarbeitung

  1. customThe product of the reaction, which
  2. customwas used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-2cf4af21d59b4536ac8eecc3f7ccc3b5
Quelldatensatz
uspto-grants-2011_09
Patentnummer
US08012997B2

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