Hydrochloric Acid → HCID 67410831, Verbindung

HRID 909210Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 909210
[ClH:1].[CH3:2][O:3][C:4](=[O:22])[C@@H:5]([NH:14]C(OC(C)(C)C)=O)[CH2:6][CH2:7][N:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>>[ClH:1].[ClH:1].[CH3:2][O:3][C:4](=[O:22])[C@@H:5]([NH2:14])[CH2:6][CH2:7][N:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 67412729HCID 67412729, Verbindung

Produkt 1

HCID 67410831HCID 67410831, VerbindungAusbeute 46 %

Versuchsvorschrift

HCl (0.45 mL of 4M in dioxane) was added to (S)-2-tert-Butoxycarbonylamino-4-piperidin-1-yl-butyric acid methyl ester and the mixture was stirred at room temperature for 2 hours. The reaction mixture was concentrated under reduced pressure and dried under high vacuum for 16 hours to provide the product (46% yield).

Aufarbeitung

  1. concentrationThe reaction mixture was concentrated under reduced pressure
  2. customdried under high vacuum for 16 hours

Quellen und Nachweise

ORD-Eintrag
ord-29b2caa72050464187c879037eab447f
Quelldatensatz
uspto-grants-2011_09
Patentnummer
US08017641B2

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