Hydrochloric Acid → HCID 86594427, Verbindung

Reaktionsgleichung

[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH:13]C(OC(C)(C)C)=O)[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8].[ClH:22]>>[ClH:22].[ClH:22].[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH2:13])[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8]

Komponenten

Edukt 2

HCID 313Hydrochloric Acid

HCID 86594426HCID 86594426, Verbindung

Produkt 1

HCID 86594427HCID 86594427, Verbindung

Versuchsvorschrift

(S)-2-tert-Butoxycarbonylamino-4-[(2-methoxyethyl)-methylamino]-butyric acid methyl ester (0.086 g, 0.28 mmol) was treated with HCl (1 mL of 4M in dioxane) and sonicated. The mixture was concentrated and dried under high vacuum to provide the product.

Aufarbeitung

customsonicated
concentrationThe mixture was concentrated
customdried under high vacuum
customto provide the product

Quellen und Nachweise

ORD-Eintrag: ord-c6b75837598e49c4b14507a8a40a53dd
Quelldatensatz: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08017641B2

Notizen zur Reaktion

Wird geladen…