HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(4-Methoxyphenyl)acetamide → {4-Bromo-2-[2-(4-methoxybenzyl)oxazol-4-yl]phenoxy}acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(4-Methoxyphenyl)acetamide | HCID 241868 | — |
| Edukt | HCID 57658801 | HCID 57658801 | — |
| Produkt | {4-Bromo-2-[2-(4-methoxybenzyl)oxazol-4-yl]phenoxy}acetic acid | HCID 57658807 | — |
Reaktionsschritte
Title compound was prepared from [4-bromo-2-(2-bromoacetyl)phenoxy]acetic acid ethyl ester and 2-(4-methoxyphenyl)acetamide according to GP5 and GP3: LC/MS (an10p8) Rt 2.40 min, m/z 418 [M+H]+; 1H NMR (CDCl3): δ 3.72 (s, 3H), 4.14 (s, 1H), 4.85 (s, 1H), 6.92 (m, 2H), 7.02 (d, 1H), 7.2 (d, 1H), 7.23 (d, 1H), 7.44 (d, 1H), 8.05 (s, 1H), 8.67 (s, 1H), 13.2 (br s, 1H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08022063B2 |
| Quelldatensatz | uspto-grants-2011_09 |
| ORD ID | ord-63f98344647e449e9b55118a89be70bd |
| Quellennotiz | uspto-grants-2011_09 |