Acetic Anhydride → N-(3,5-dimethoxyphenyl)acetamide

Beteiligte Stoffe

Reaktionsschritte

To a solution of 3,5-dimethoxy-phenylamine (22.0 g, 143.6 mmol) in toluene (100 mL), is added slowly Ac2O (14 mL) at room temperature. After stirring 30 minutes, hexane (50 mL) is added with stirring at room temperature. The resulting solid is filtered and washed with hexane (50 mL) to offer designed product as a white solid 14.

Herkunft & Nachweise