Aniline → HCID 67396451, Verbindung
Reaktionsgleichung
[C:1]([CH2:4][C:5]1[N:6]=[C:7]([S:10][C:11]([CH3:16])([CH3:15])[C:12]([OH:14])=[O:13])[S:8][CH:9]=1)([OH:3])=O.[NH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.FC(F)(F)C(O)=O>>[NH:17]([C:1](=[O:3])[CH2:4][C:5]1[N:6]=[C:7]([S:10][C:11]([CH3:16])([CH3:15])[C:12]([OH:14])=[O:13])[S:8][CH:9]=1)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1Komponenten
4
Versuchsvorschrift
The title yellow resin (2.9 g) was obtained using 2-{[4-(carboxymethyl)-1,3-thiazol-2-yl]thio}-2-methylpropionic acid resin synthesized in Example 461-4 and aniline as starting materials and by an operation similar to that of Example 461-5. A part of the resin was cleaved with trifluoroacetic acid and the structure was confirmed.
Quellen und Nachweise
- ORD-Eintrag
- ord-8c47f95f531147c380abb2891dcb90bf
- Quelldatensatz