Hydrazine → HCID 27055575, Verbindung
Reaktionsgleichung
[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([O:14]CC)=O.[NH2:17][NH2:18]>C(O)C>[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([NH:17][NH2:18])=[O:14]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A solution of 90 (2.0 g, 9.12 mmol) and hydrazine (5.1 g, 91 mmol) in ethanol (30 mL) was heated at reflux overnight. The mixture was concentrated under reduced pressure to give 91 (1.87 g ˜100%) which was used without further purification.
Aufarbeitung
- temperatureat reflux overnight
- concentrationThe mixture was concentrated under reduced pressure
Quellen und Nachweise
- ORD-Eintrag
- ord-62c165ed74a74b769d7b88b2dc611239
- Quelldatensatz
- uspto-grants-2007_09
- Patentnummer
- US07265122B2
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