2-Methoxyethylamine → HCID 136333264, Verbindung

HRID 915946Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 915946
Br[C:2]1[CH:7]=[CH:6][C:5]([C:8]2[NH:9][C:10](=[O:24])[C:11]3[C:16]([CH:17]4[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]4)=[N:15][N:14]([CH3:23])[C:12]=3[N:13]=2)=[C:4]([O:25][CH2:26][CH3:27])[CH:3]=1.[CH3:28][O:29][CH2:30][CH2:31][NH2:32]>>[CH:17]1([C:16]2[C:11]3[C:10](=[O:24])[NH:9][C:8]([C:5]4[CH:6]=[CH:7][C:2]([NH:32][CH2:31][CH2:30][O:29][CH3:28])=[CH:3][C:4]=4[O:25][CH2:26][CH3:27])=[N:13][C:12]=3[N:14]([CH3:23])[N:15]=2)[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1

Komponenten

3

Edukt 2

HCID 80182-MethoxyethylamineHCID 136005963HCID 136005963, Verbindung

Produkt 1

HCID 136333264HCID 136333264, VerbindungAusbeute 31 %

Versuchsvorschrift

The same reaction procedure as in Example 27 was performed, except that the compound obtained in Example 85 was used in place of the compound obtained in Example 26, and 2-methoxyethylamine was used in place of N-methylpiperazine. In this manner, 46 mg (31%) of the captioned compound was obtained.

Aufarbeitung

  1. customThe same reaction procedure as in Example 27

Quellen und Nachweise

ORD-Eintrag
ord-99e2e632b0e54b119fe682e5576fb42d
Quelldatensatz
uspto-grants-2007_09
Patentnummer
US07268128B2

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