Benzylamine → HCID 86733699, Verbindung

HRID 918203Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 918203
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:9][C:10]1[C:15]([C:16]([CH3:19])([CH3:18])[CH3:17])=[CH:14][C:13]([CH:20]([CH3:24])[C:21](Cl)=[O:22])=[CH:12][C:11]=1[C:25]([CH3:28])([CH3:27])[CH3:26]>CCCCCCC>[CH2:1]([NH:8][C:21](=[O:22])[CH:20]([C:13]1[CH:14]=[C:15]([C:16]([CH3:17])([CH3:18])[CH3:19])[C:10]([OH:9])=[C:11]([C:25]([CH3:28])([CH3:27])[CH3:26])[CH:12]=1)[CH3:24])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Komponenten

4

Edukt 2

HCID 7504BenzylamineHCID 198301384-Hydroxy-3,5-di-tert.-butylphenyl-propionic acid-chloride

Produkt 1

HCID 86733699HCID 86733699, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8900HeptaneLösungsmittel2×

Versuchsvorschrift

To a solution of 22.4 g of benzyl amine (0.21 mol) in 100 ml of heptane 29.6 g of 4-hydroxy-3,5-di-tert.-butylphenyl-propionic acid-chloride (0.1 mol) -- dissolved in 200 ml of heptane -- were added dropwise at 20°C, then the solution was boiled under reflux for 3 hours. Working up followed in the manner described in Example 12.

Aufarbeitung

  1. additionwere added dropwise at 20°C
  2. temperatureunder reflux for 3 hours

Quellen und Nachweise

ORD-Eintrag
ord-2524b7ffb2254c94aa27e5f042fbd9f2
Quelldatensatz
uspto-grants-1976_07
Patentnummer
US03969530

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