Benzene → N,N-diethyl 3,7,11-trimethyldodeca-2,4,10-trienylamine

HRID 918332Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 918332
Cl[C:2]([CH3:17])([CH3:16])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:15])[CH2:7][CH:8]=[CH:9][C:10]([CH3:14])=[CH:11][CH2:12]Br.BrCC=C(C)C=CCC(C)CCC=C(C)C.C1C=CC=CC=1.[CH2:40]([NH:42][CH2:43][CH3:44])[CH3:41]>C(Cl)Cl>[CH2:40]([N:42]([CH2:12][CH:11]=[C:10]([CH3:14])[CH:9]=[CH:8][CH2:7][CH:6]([CH3:15])[CH2:5][CH2:4][CH:3]=[C:2]([CH3:17])[CH3:16])[CH2:43][CH3:44])[CH3:41]

Komponenten

6

Edukt 4

HCID 241BenzeneHCID 8021DiethylamineHCID 5387143211-Chloro-3,7,11-trimethyldodeca-2,4-dienyl bromideHCID 54370561HCID 54370561, Verbindung

Produkt 1

HCID 53837124N,N-diethyl 3,7,11-trimethyldodeca-2,4,10-trienylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Versuchsvorschrift

Five grams of 1 bromo-3,7,11-trimethyldodeca-2,4,10-triene in 25 ml. of benzene is mixed with 4 g. of diethylamine and the mixture stirred for about three hours. Methylene chloride (50 ml.) is added and the mixture washed with dilute sodium hydroxide and then water and evaporated to yield N,N-diethyl 3,7,11-trimethyldodeca-2,4,10-trienylamine.

Aufarbeitung

  1. washthe mixture washed with dilute sodium hydroxide
  2. customwater and evaporated

Quellen und Nachweise

ORD-Eintrag
ord-fd1ec86af4c24fd3b2e9cc477e948b13
Quelldatensatz
uspto-grants-1976_07
Patentnummer
US03970704

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