Benzyl Chloride → 3-Benzyl-2,2,5,5-tetramethyl-4-oxo-imidazolidine
Reaktionsgleichung
[CH3:1][C:2]1([CH3:10])[NH:6][C:5](=[O:7])[C:4]([CH3:9])([CH3:8])[NH:3]1.[CH2:11](Cl)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([N:6]1[C:5](=[O:7])[C:4]([CH3:9])([CH3:8])[NH:3][C:2]1([CH3:10])[CH3:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1Komponenten
3
Versuchsvorschrift
If, instead of 7,14-diaza-15-oxo-dispiro[5.1.5.2]pentadecane, 2,2,5,5-tetramethyl-4-oxo-imidazolidine is used, and this alkylated with benzyl chloride as described in Example 1, then 3-benzyl-2,2,5,5-tetramethyl-4-oxo-imidazolidine (VII), M.P. 210°C, is obtained.
Quellen und Nachweise
- ORD-Eintrag
- ord-0b39d41fc52a4d9daba8b65d702fd22b
- Quelldatensatz
- uspto-grants-1976_07
- Patentnummer
- US03971757
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