HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Iodide → 3-Cyclopentyloxy-4-methoxybenzyl alcohol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Iodide | HCID 5238 | — |
| Edukt | Cesium carbonate | HCID 10796 | — |
| Edukt | 3-Hydroxy-4-methoxybenzyl alcohol | HCID 78089 | — |
| Edukt | Cyclopentyloxy-bromide | HCID 21697665 | — |
| Produkt | 3-Cyclopentyloxy-4-methoxybenzyl alcohol | HCID 11138706 | 35,8% |
Reaktionsschritte
From 3-hydroxy-4-methoxybenzyl alcohol (50 g, 0.324 mol), cyclopentyloxybromide (70 ml, 0.648 mol), caesium carbonate (72.83 g, 0.222 mol) and sodium iodide (5.63 g, 0.037 mol). Chromatography (SiO2 ; EtOAc-C6H14, 1:3) to yield the title compound (25.782 g). (Found C, 69.92; H, 8.18. C13H18O3 requires C, 70.25; H, 8.16).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05723460 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-96b5709519a5432ab5539f7faa641c73 |
| Quellennotiz | uspto-grants-1998_03 |