Tert-Butyl 4-(3-(Tert-Butyldisulfanyl)-2-(Isobutoxycarbonylamino)Propanamido)Piperidine-1-Carboxylate → Isobutyl 3-(Isopropyldisulfanyl)-1-Oxo-1-(Piperidin-4-ylamino)Propan-2-ylcarbamate
Reaktionsgleichung
[C:1]([S:5][S:6][CH2:7][CH:8]([NH:25][C:26]([O:28][CH2:29][CH:30]([CH3:32])[CH3:31])=[O:27])[C:9]([NH:11][CH:12]1[CH2:17][CH2:16][N:15](C(OC(C)(C)C)=O)[CH2:14][CH2:13]1)=[O:10])(C)([CH3:3])[CH3:2]>Cl.O1CCOCC1>[CH:1]([S:5][S:6][CH2:7][CH:8]([NH:25][C:26](=[O:27])[O:28][CH2:29][CH:30]([CH3:32])[CH3:31])[C:9](=[O:10])[NH:11][CH:12]1[CH2:13][CH2:14][NH:15][CH2:16][CH2:17]1)([CH3:3])[CH3:2]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To the compound from Example 60 (7.085 g, 18.12 mmol) was added 30 ml of 4M HCl/Dioxane. The reaction was completed after 2 h at RT. The title compound was used for the next step without further purification.