HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorodiisopropylphosphine → HCID 178460690, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorodiisopropylphosphine | HCID 538967 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Edukt | HCID 178440935 | HCID 178440935 | — |
| Produkt | HCID 178460690 | HCID 178460690 | — |
Reaktionsschritte
Procedure as described for NP Amidine I using the following amounts: 1.54 g of 4-tert-butyl-N1-(2-tert-butylphenyl)benzamidine (Amidine VII, 5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.80 mL chlorodiisopropylphosphine (5.0 mmol). After filtration to remove lithium chloride and removal of solvent, a yellow semi-solid was isolated (1.9 g, 100%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09283555B2 |
| Quelldatensatz | uspto-grants-2016_03 |
| ORD ID | ord-a7d2b1ae01704f778ef8d11870c35a07 |
| Quellennotiz | uspto-grants-2016_03 |