Trifluoroacetic acid → HCID 62329121, Verbindung

HRID 926384Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 926384
Cl.[CH:2]1([CH2:5][O:6][CH:7]2[CH2:11][CH2:10][NH:9][CH2:8]2)[CH2:4][CH2:3]1.FC(F)(F)C(O)=O>>[CH2:5]([O:6][CH:7]1[CH2:11][CH2:10][NH:9][CH2:8]1)[CH:2]([CH3:4])[CH3:3]

Komponenten

3

Edukt 2

HCID 6422Trifluoroacetic acidHCID 45075448HCID 45075448, Verbindung

Produkt 1

HCID 62329121HCID 62329121, Verbindung

Versuchsvorschrift

The compound as its trifluoroacetic acid salt was obtained from (S)-3-hydroxy-pyrrolidine-1-carboxylic acid tert-butyl ester following a reaction sequence according to the synthesis of comp. no. 22a. Trifluoroacetic acid was used instead of hydrogen chloride in the final deprotection. LC/MS (method 5): Rt=0.78 min; m/z=144.2 (M+H+).

Aufarbeitung

  1. customaccording to the synthesis of comp

Quellen und Nachweise

ORD-Eintrag
ord-cd698441b8e24480b890565374e4a2f3
Quelldatensatz
uspto-grants-2016_03
Patentnummer
US09284333B2

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