4-Methanesulfonyl-2-methylbutan-2-amine → HCID 71105733, Verbindung

HRID 927814

Reaktionsgleichung

Reaktionsgleichung von HRID 927814
[CH:1]1([C:4]2[CH:5]=[CH:6][C:7]([C:15]([OH:17])=O)=[N:8][C:9]=2[O:10][CH2:11][CH:12]2[CH2:14][CH2:13]2)[CH2:3][CH2:2]1.[CH3:18][C:19]([NH2:27])([CH2:21][CH2:22][S:23]([CH3:26])(=[O:25])=[O:24])[CH3:20]>>[CH3:26][S:23]([CH2:22][CH2:21][C:19]([NH:27][C:15]([C:7]1[CH:6]=[CH:5][C:4]([CH:1]2[CH2:2][CH2:3]2)=[C:9]([O:10][CH2:11][CH:12]2[CH2:13][CH2:14]2)[N:8]=1)=[O:17])([CH3:20])[CH3:18])(=[O:25])=[O:24]

Komponenten

3

Edukt 2

HCID 545958664-Methanesulfonyl-2-methylbutan-2-amineHCID 710873465-Cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid

Produkt 1

HCID 71105733HCID 71105733, Verbindung

Versuchsvorschrift

The title compound was synthesized in analogy to Example 1, using 5-cyclopropyl-6-cyclopropylmethyloxy-pyridine-2-carboxylic acid (Example 42a) and 2-methyl-4-(methylsulfonyl)-2-butanamine (CAN 1250515-16-2) as starting materials; LC-MS (UV peak area/ESI) 95%, 381.1843 (M+H)+.

Quellen und Nachweise

ORD-Eintrag
ord-2e00b6d28d4e454b97f4fd8167be068f
Quelldatensatz
uspto-grants-2016_03
Patentnummer
US09290451B2

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