Dichloromethane → HCID 58081285, Verbindung
Reaktionsgleichung
[O:1]=[S:2]1(=[O:13])[CH2:6][CH2:5][C:4]2[CH:7]=[C:8]([CH2:11][OH:12])[CH:9]=[CH:10][C:3]1=2.C(Cl)Cl>>[O:1]=[S:2]1(=[O:13])[CH2:6][CH2:5][C:4]2[CH:7]=[C:8]([CH2:11][O:12][S:2]([CH3:3])(=[O:13])=[O:1])[CH:9]=[CH:10][C:3]1=2Komponenten
3
Versuchsvorschrift
To a solution of (1,1-Dioxo-2,3-dihydro-1H-1lambda*6*-benzo[b]thiophen-5-yl)-methanol (crude, 160 mg, 0.64 mmol) and triethylamne (180 ul, 1.29 mmol) in DCM (7 ml) Methanesulfonylchloride (60 ul, 0.77 mmol) was added at rt. The reaction mixture was stirred at it for 3 hours.
Quellen und Nachweise
- ORD-Eintrag
- ord-d527cf76fa4b4b75a7248d1d8db795d9
- Quelldatensatz
- uspto-grants-2016_03
- Patentnummer
- US09290485B2
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