4-(Trifluoromethyl)aniline → 4-(4-Trifluoromethylphenylaminosulfonyl)-5-methylisoxazole

HRID 962803

Reaktionsgleichung

Reaktionsgleichung von HRID 962803
FC(F)(F)C1C=CC(NS(C(C)=COCC)(=O)=O)=CC=1.[F:21][C:22]([F:31])([F:30])[C:23]1[CH:29]=[CH:28][C:26]([NH2:27])=[CH:25][CH:24]=1.Cl[S:33]([C:36]1[CH:37]=[N:38][O:39][C:40]=1[CH3:41])(=[O:35])=[O:34]>>[F:21][C:22]([F:30])([F:31])[C:23]1[CH:29]=[CH:28][C:26]([NH:27][S:33]([C:36]2[CH:37]=[N:38][O:39][C:40]=2[CH3:41])(=[O:35])=[O:34])=[CH:25][CH:24]=1

Komponenten

4

Edukt 3

HCID 99644-(Trifluoromethyl)anilineHCID 27761415-Methyl-1,2-oxazole-4-sulfonyl chlorideHCID 569825522-(4-Trifluoromethylphenylaminosulfonyl)1-ethoxypropene

Produkt 1

HCID 570891944-(4-Trifluoromethylphenylaminosulfonyl)-5-methylisoxazole

Versuchsvorschrift

AA16 was prepared starting from 2-(4-trifluoromethylphenylaminosulfonyl)1-ethoxypropene under the same conditions as described for AA11. Alternatively, AA16 was prepared from 4-trifluoromethylaniline and 4-chlorosulfonyl-5-methylisoxazole.

Aufarbeitung

  1. customAA16 was prepared

Quellen und Nachweise

ORD-Eintrag
ord-dc4e9641eb91427b9dcb45310c5bab47
Quelldatensatz
uspto-grants-1998_06
Patentnummer
US05760066

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