1,2-Dichlorohexafluorocyclobutane → 1-Chloro 3,3,4,4-tetrafluoro cyclobutene

HRID 963798

Reaktionsgleichung

Reaktionsgleichung von HRID 963798
[Cl:1][C:2]1(F)[C:5]([F:7])([F:6])[C:4]([F:9])([F:8])[C:3]1(F)Cl.FC1(F)C(F)=C(F)C1(F)F>>[F:6][C:5]1([F:7])[C:2]([Cl:1])=[CH:3][C:4]1([F:9])[F:8]

Komponenten

3

Edukt 2

HCID 96431,2-DichlorohexafluorocyclobutaneHCID 12767Hexafluorocyclobutene

Produkt 1

HCID 126638541-Chloro 3,3,4,4-tetrafluoro cyclobutene

Versuchsvorschrift

The conversion of 1,2-dichlorohexafluorocyclobutane was 30%, the selectivity of the targeted hexafluorocyclobutene was 96% and a 3.5% selectivity of tetrafluoro-1-chlorocyclobutene was formed as the by-product. The selectivity and the conversion were calculated by multiplying the correction coefficient, which was independently determined by the gas chromatography peak areas. The same procedure was used for the following operations.

Quellen und Nachweise

ORD-Eintrag
ord-aba3804530b64007a937b59926300bb1
Quelldatensatz
uspto-grants-1998_06
Patentnummer
US05763703

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