2-Butanethiol → Di-sec-butyl disulfide

HRID 964720Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 964720
[CH3:1][CH:2]([SH:5])[CH2:3][CH3:4]>C(#N)C>[CH3:1][CH:2]([S:5][S:5][CH:2]([CH3:1])[CH2:3][CH3:4])[CH2:3][CH3:4]

Komponenten

3

Versuchsvorschrift

A solution of 150 μg of LL-E33288γ1 -I in 1 ml of acetonitrile was treated with 50 μl of a 1 μmole/ml solution of 1-methyl-1-propyl mercaptan. After 2 hours, the reaction was complete, giving the desired 1-methyl-1-propyl disulfide of LL-E33288γ1 -I.

Quellen und Nachweise

ORD-Eintrag
ord-08b99e5042f94465aecce77924bc62ef
Quelldatensatz
uspto-grants-1998_06
Patentnummer
US05770710

Notizen zur Reaktion

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