HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 964927Erstellt: 26. Oktober 2026
(3,5-Di-tert-butylphenyl)methanol → 3,5-Bis(tert-butyl)benzaldehyde
https://huagongshe.com/reaction/964927
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | (3,5-Di-tert-butylphenyl)methanol | HCID 12660843 | — |
| Katalysator | Manganese dioxide | HCID 14801 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 3,5-Bis(tert-butyl)benzaldehyde | HCID 1268253 | — |
Reaktionsschritte
To the crude alcohol from above was added MnO2 and CHCl3 (20 mL). The mixture was stirred overnight at 25° C. and filtered, and the organic solvent was evaporated. The crude residue was purified by flash chromatography on silica gel eluting with 1:6 ethyl acetate-hexane to give 0.3 g of 3,5-di-t-butylbenzaldehyde as a white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05773421 |
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| Quelldatensatz | uspto-grants-1998_06 |
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| ORD ID | ord-18eedb25bce74f04b968f52632084159 |
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| Quellennotiz | uspto-grants-1998_06 |
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