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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 964927Erstellt: 26. Oktober 2026

(3,5-Di-tert-butylphenyl)methanol → 3,5-Bis(tert-butyl)benzaldehyde

https://huagongshe.com/reaction/964927

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(3,5-Di-tert-butylphenyl)methanolHCID 12660843—
KatalysatorManganese dioxideHCID 14801—
LösungsmittelChloroformHCID 6212—
Produkt3,5-Bis(tert-butyl)benzaldehydeHCID 1268253—

Reaktionsbedingungen

Temperatur25 °C

Reaktionsschritte

To the crude alcohol from above was added MnO2 and CHCl3 (20 mL). The mixture was stirred overnight at 25° C. and filtered, and the organic solvent was evaporated. The crude residue was purified by flash chromatography on silica gel eluting with 1:6 ethyl acetate-hexane to give 0.3 g of 3,5-di-t-butylbenzaldehyde as a white solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05773421
Quelldatensatzuspto-grants-1998_06
ORD IDord-18eedb25bce74f04b968f52632084159
Quellennotizuspto-grants-1998_06