Ethyl alpha-benzylacetoacetate → HCID 178433370, Verbindung

Beteiligte Stoffe

Reaktionsschritte

A mixture of ethyl 2-benzyl-3-oxobutanoate (6 g, 27.2 mmol), guanidine carbonate (2.94 g, 16.3 mmol) and ethanol (20 ml) was refluxed for 10 hours. After cooling, the precipitate was filtered and washed with water, ethanol and ether in order, to the object compound (3.62 g, 61.7%).

Herkunft & Nachweise