HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Hydroxyhexanoic acid → 5-Butyloxazolidine-2,4-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Hydroxyhexanoic acid | HCID 99824 | — |
| Edukt | Hexanamide, 2-hydroxy- | HCID 9833961 | — |
| Edukt | 5-Butyl-oxazolidin-2,4-dione sodium salt | HCID 69745152 | — |
| Produkt | 5-Butyloxazolidine-2,4-dione | HCID 9942204 | — |
Reaktionsschritte
A part of the reaction solution was sampled and the components of the reaction solution were analyzed by HPLC, as a result, the concentration of the starting material 2-hydroxyhexanoic acid amide was 1.6 mass % in the solution, the concentration of 5-butyl-oxazolidin-2,4-dione sodium salt as the objective product was 24.0 mass % in the solution and the concentration of 2-hydroxyhexanoic acid was 2.3 mass % in the solution. From these analysis values, the conversion of 2-hydroxyhexanoic acid amide was 92.6% and the yield in terms of 5-butyl-oxazolidin-2,4-dione was 82.1%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06953859B2 |
| Quelldatensatz | uspto-grants-2005_10 |
| ORD ID | ord-ff9ac95875e74c2f847a4266786d5038 |
| Quellennotiz | uspto-grants-2005_10 |