HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Methoxide → [2-Methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Methoxide | HCID 10942334 | — |
| Edukt | 1-Benzoyl-3-[2-methoxy-5-(tetrahydropyran-4-yl)-phenyl]-thiourea | HCID 22719571 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | [2-Methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea | HCID 22015747 | — |
Reaktionsschritte
To a solution of 1-benzoyl-3-[2-methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea (X) in methanol is added sodium methylate solution and stirring continued for about 1 h at room temperature. The product (XI) [2-methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea is isolated by conventional means.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07304058B2 |
| Quelldatensatz | uspto-grants-2007_12 |
| ORD ID | ord-a782e1606e434c12b23ef122ad852623 |
| Quellennotiz | uspto-grants-2007_12 |