6-Ethylnicotinonitrile → 3-Pyridinecarbonitrile, 2-ethyl-6-methyl-
Reaktionsgleichung
[CH3:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[C:4]([CH:10]=[CH2:11])[N:3]=1.C(C1C=CC(C#N)=CN=1)C>>[CH2:10]([C:4]1[N:3]=[C:2]([CH3:1])[CH:9]=[CH:8][C:5]=1[C:6]#[N:7])[CH3:11]Komponenten
3
Versuchsvorschrift
Compound 386B was prepared from 386A by a route analogous to that used for the preparation of 384B. HPLC retention time=1.18 min. (Condition A), M+=147.
Quellen und Nachweise
- ORD-Eintrag
- ord-6ea5a59e541946329d8a9fb9b90b2f82
- Quelldatensatz
- uspto-grants-2007_12
- Patentnummer
- US07312209B2
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