HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 3-formyl-1H-indole-7-carboxylate → Methyl 3-(hydroxyiminomethyl)indole-7-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 3-formyl-1H-indole-7-carboxylate | HCID 762965 | — |
| Edukt | Hydroxyammonium hydrochloride | HCID 22029257 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Methyl 3-(hydroxyiminomethyl)indole-7-carboxylate | HCID 136376389 | 97,4% |
Reaktionsschritte
5 g of methyl 3-formylindole-7-carboxylate (0.024 mol) are added to a solution of 0.03 mol of hydroxylammonium hydrochloride in dimethylformamide. The reaction mixture is heated at 125° for one hour and subjected to conventional work-up, giving 5.1 g of methyl 3-(hydroxyiminomethyl)indole-7-carboxylate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07312342B2 |
| Quelldatensatz | uspto-grants-2007_12 |
| ORD ID | ord-35682b06232f4d1fb4ecb9fe1e25772f |
| Quellennotiz | uspto-grants-2007_12 |