HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glutaric anhydride → Phthalic Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glutaric anhydride | HCID 7940 | — |
| Edukt | 4-Aminophthalic acid | HCID 72912 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | Phthalic Acid | HCID 1017 | — |
Reaktionsschritte
65.1 g (0.36 mol) of 4-aminophthalic acid in 500 ml of dioxane are reacted with 43.12 g (0.38 mol) of glutaric anhydride, in the manner described in Example 9, to give 4-glutaramidyl)-phthalic acid, and the latter is subsequently cyclised. 70 g (75% of theory) of 4-(glutarimidyl)-phthalic anhydride of melting point 220°-222° C. are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04160081 |
| Quelldatensatz | uspto-grants-1979_07 |
| ORD ID | ord-fec00bd137a440758e615126cce69ed4 |
| Quellennotiz | uspto-grants-1979_07 |