Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Nitrobenzene | HCID 7416 | — |
| Edukt | p-Toluidine | HCID 7813 | — |
| Edukt | Potassium Acetate | HCID 517044 | — |
| Edukt | Selenium | HCID 6326970 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 1-(4-Methylphenyl)-3-phenylurea | HCID 572170 | — |
Reaktionsschritte
Ten milliliters of nitrobenzene, 100 milliliters of tetrahydrofuran, 1.0 gram potassium acetate, 1.0 gram selenium and 21.4 grams of p-toluidine are charged to the autoclave which is then flushed and pressured to 800 psig with carbon monoxide. The temperature is raised to 180° C. for one hour giving 1-p-tolyl-3-phenylurea as product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04052454 |
|---|
| Quelldatensatz | uspto-grants-1977_10 |
|---|
| ORD ID | ord-18802182db8c4af2ae36e5ffa8b87fbd |
|---|
| Quellennotiz | uspto-grants-1977_10 |
|---|
