HCID 13066945, Verbindung → 2-Methyl-3-hydroxy-4-formyl-5-vinylpyridine
Reaktionsgleichung
[CH3:1][C:2]1[C:7]([OH:8])=[C:6]([CH2:9][OH:10])[C:5]([CH:11]=[CH2:12])=[CH:4][N:3]=1>[O-2].[O-2].[Mn+4].C(Cl)(Cl)Cl>[CH3:1][C:2]1[C:7]([OH:8])=[C:6]([CH:9]=[O:10])[C:5]([CH:11]=[CH2:12])=[CH:4][N:3]=1Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
A solution of 10 g. of 2-methyl-3-hydroxy-4-hydroxymethyl-5-vinylpyridine in 300 ml. of hot chloroform was treated with 100 g. of manganese dioxide. After 1/2 hour of stirring, the mixture was filtered and the filtrate was evaporated to dryness to give 2-methyl-3-hydroxy-4-formyl-5-vinylpyridine.
Aufarbeitung
- filtrationthe mixture was filtered
- customthe filtrate was evaporated to dryness
Quellen und Nachweise
- ORD-Eintrag
- ord-c560a986c5e74c1a9976da70231bd9e9
- Quelldatensatz
- uspto-grants-1977_10
- Patentnummer
- US04053606
Notizen zur Reaktion
Wird geladen…