HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → 4-Methylhexylmethylmalonic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Diethyl 4-methylhexylmethylmalonate | HCID 54113602 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-Methylhexylmethylmalonic acid | HCID 54000156 | — |
Reaktionsschritte
First, 8.18 g (0.22 mol) of sodium hydroxide was dissolved in a mixture solution of 28 ml of water and 14 ml of methanol, thus forming a solution. Next, g of the crude product (II), not refined, was added to the resultant solution and reacted with the solution at 20° C. for three to five hours, thereby obtaining 18.4 g of 4-methylhexylmethylmalonic acid (III). This reaction is represented as follows: ##STR4##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05063058 |
| Quelldatensatz | uspto-grants-1991_11 |
| ORD ID | ord-940c9a4c925c424b8d6bdebca07d15d3 |
| Quellennotiz | uspto-grants-1991_11 |