Thionyl Chloride → [3-(Trifluoromethyl)phenoxy]acetyl chloride

HRID 973719Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 973719
[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][CH:13]=1)[O:6][CH2:7][C:8](O)=[O:9].S(Cl)([Cl:18])=O>>[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][CH:13]=1)[O:6][CH2:7][C:8]([Cl:18])=[O:9]

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 19914302-[3-(Trifluoromethyl)phenoxy]acetic acid

Produkt 1

HCID 13140641[3-(Trifluoromethyl)phenoxy]acetyl chloride

Versuchsvorschrift

A solution of 6 g of the product of Step B in 36 ml of thionyl chloride was refluxed with stirring for one hour and was evaporated to dryness under reduced pressure to obtain 6.44 g of the desired product which was used as is for the next step.

Aufarbeitung

  1. customwas evaporated to dryness under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-c09db5187a1f4a44a6e4420e23b35327
Quelldatensatz
uspto-grants-1991_11
Patentnummer
US05064861

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