Benzyl Alcohol → HCID 19972025, Verbindung

Reaktionsgleichung

[C:1]([O:5][C:6]([NH:8][CH2:9][P:10]([CH2:13][NH:14][C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16])(=[O:12])[OH:11])=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:22](O)[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[C:1]([O:5][C:6]([NH:8][CH2:9][P:10]([CH2:13][NH:14][C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16])(=[O:11])[O:12][CH2:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Komponenten

Edukt 2

HCID 244Benzyl Alcohol

HCID 11120883HCID 11120883, Verbindung

Produkt 1

HCID 19972025HCID 19972025, VerbindungAusbeute 55 %

Versuchsvorschrift

In analogy to Example 4, the benzyl phosphinate 5 was prepared from the phosphinic acid 1 and benzyl alcohol in a yield of 55%.

Quellen und Nachweise

ORD-Eintrag: ord-61ff1298860e48d5867f06d2ee3b7a68
Quelldatensatz: uspto-grants-1997_03
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05608098

Notizen zur Reaktion

Wird geladen…