HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 15230549, Verbindung → 9-Aminononanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 15230549 | HCID 15230549 | — |
| Katalysator | Lindlars catalyst | HCID 131709914 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 9-Aminononanoic acid | HCID 136877 | — |
Reaktionsschritte
9-Azido-nonanoic acid (2.83 g, 14.2 mmol) was dissolved in ethanol (30 mL) and Lindlar catalyst (300 mg) added. The solution was hydrogenated at 50 psi, 30° C. for 4 hours, after which the catalyst was removed by filtration through Kieselguhr, washing with methanol. The solvent was removed in vacuo to give a pale yellow solid, 1.7 g (70%);
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05610145 |
| Quelldatensatz | uspto-grants-1997_03 |
| ORD ID | ord-4be2edef1fd94a7181ae9cdef2e4679d |
| Quellennotiz | uspto-grants-1997_03 |