Hydrochloric Acid → HCID 178501833, Verbindung

HRID 976257Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 976257
[ClH:1].[NH2:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([O:9][CH2:10][C:11]([O:13][C:14](C)(C)C)=[O:12])[CH2:5][CH2:4]1>CO>[ClH:1].[NH2:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([O:9][CH2:10][C:11]([O:13][CH3:14])=[O:12])[CH2:5][CH2:4]1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 178451370HCID 178451370, Verbindung

Produkt 1

HCID 178501833HCID 178501833, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrochloric acid gas is piped for an hour over a solution of 59.4 g of tert.butyl (trans-4-aminocyclohexyl)oxyacetate in 500 ml of methanol, cooled in an ice bath, and then the mixture is stirred overnight at ambient temperature. It is evaporated to dryness, the residue is triturated with acetone and the solid is suction filtered and dried.

Aufarbeitung

  1. temperaturecooled in an ice bath
  2. customIt is evaporated to dryness
  3. customthe residue is triturated with acetone
  4. filtrationfiltered
  5. customdried

Quellen und Nachweise

ORD-Eintrag
ord-78f9cc1f0fb44aff9dfe05c9f3b79710
Quelldatensatz
uspto-grants-1997_03
Patentnummer
US05612335

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