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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 976898Erstellt: 24. Oktober 2026

Decyl chloroformate → Phthalimide hydrochloride

https://huagongshe.com/de/reaction/976898

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDecyl chloroformateHCID 108727—
EduktN-[2-[4-(6-fluoro1H-indazol-3-yl)-1-piperazinyl]ethyl]phthalimideHCID 18467209—
LösungsmittelDiethyl EtherHCID 3283—
ProduktPhthalimide hydrochlorideHCID 22266261—

Reaktionsschritte

A mixture of decanyl chloroformate (2.4 g, 11 mmol), and N-[2-[4-(6-fluoro-1H-indazol-3-yl)-1-piperazinyl]ethyl]phthalimide (3.9 g, 10 mmol) was warmed on the steam bath for 15 minutes. The reaction was allowed to cool to ambient temperature, and then ether was added to the residue. The resulting solid was filtered to afford N2-[4-(1 -decanoxy-6-fluoro-1H-indazol-3-yl)-1-piperazinyl]ethyl]phthalimide hydrochloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05612343
Quelldatensatzuspto-grants-1997_03
ORD IDord-94eabb6893cd4ead8af84e723c17a62a
Quellennotizuspto-grants-1997_03