HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate → 4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate | HCID 19965620 | — |
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Produkt | 4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol | HCID 54568002 | — |
Reaktionsschritte
Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate was reduced with lithium aluminum hydride in the same manner as in Reference Example 12 to yield 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol, which was then recrystallized from ethyl acetate-hexane to yield colorless plates having a melting point of 103°-104° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05614544 |
| Quelldatensatz | uspto-grants-1997_03 |
| ORD ID | ord-75b253952b1443f8887904166dc53a19 |
| Quellennotiz | uspto-grants-1997_03 |