HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-nitrophenol sodium salt → Tri(4-nitrophenoxy)tri(phenoxy)cyclotriphosphazene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-nitrophenol sodium salt | HCID 13214 | — |
| Edukt | Trichlorotriphenoxycyclotriphosphazene | HCID 23418754 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | Tri(4-nitrophenoxy)tri(phenoxy)cyclotriphosphazene | HCID 14274513 | — |
Reaktionsschritte
This material is obtained as a white solid by the treatment of sodium and phenol with hexachlorocyclotriphosphazene at -78° C. to produce the trichlorotriphenoxycyclotriphosphazene, according to D. Dell et al., J. Chem. Soc., 4072 (1965), which is incorporated herein by reference. This material is further reacted with sodium 4-nitrophenoxide in refluxing tetrahydrofuran to give the title compound in good yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04668589 |
| Quelldatensatz | uspto-grants-1987_05 |
| ORD ID | ord-076b72045e604f3193e8079edc061026 |
| Quellennotiz | uspto-grants-1987_05 |