HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → Chromium (II) bis(2-ethylhexanoate)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 2-Ethylhexanoic Acid | HCID 8697 | — |
| Edukt | chromium(II) dichloride | HCID 10197677 | — |
| Lösungsmittel | Heptane | HCID 8900 | — |
| Produkt | Chromium (II) bis(2-ethylhexanoate) | HCID 21922276 | — |
Reaktionsschritte
Chromium (II) bis(2-ethylhexanoate) is prepared by the addition of an equimolar mixture of triethylamine and 2-ethylhexanoic acid in heptane to a suspension of 0.5 mole anhydrous chromium (II) chloride in heptane. A slow reaction results in the formation of a deep purple solution and the precipitation of triethylammonium hydrochloride. The product is isolated as a purple oil after removal of the precipitate by filtration and the volatiles under vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04668838 |
| Quelldatensatz | uspto-grants-1987_05 |
| ORD ID | ord-d2533a5280b044d7bc482e2666c224f8 |
| Quellennotiz | uspto-grants-1987_05 |