Hydrogen Peroxide → Hydrogen Peroxide

HRID 979749Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 979749
[C:1]([NH:12][CH2:13][C:14]([OH:16])=[O:15])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[OH:17][OH:18]>CS(O)(=O)=O>[C:1]([NH:12][CH2:13][C:14]([O:16][OH:17])=[O:15])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:1]([NH:12][CH2:13][C:14]([OH:16])=[O:15])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[OH:17][OH:18]

Komponenten

6

Edukt 2

HCID 784Hydrogen PeroxideHCID 1712391N-(1-Oxodecyl)glycine

Produkt 3

HCID 784Hydrogen PeroxideHCID 1712391N-(1-Oxodecyl)glycineHCID 53638750HCID 53638750, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6395Methanesulfonic AcidLösungsmittel2×

Versuchsvorschrift

N-Decanoylaminoperoxyacetic acid was prepared by reaction of N-decanoylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 22.9 g (0.100 mol) of N-decanoylglycine and 17.0 g (0.500 mol) of hydrogen peroxide in 50 mL methanesulfonic acid was obtained 22.4 g of peroxyacid having an AvO of 6.06% (theoretical yield=24.5 g having an AvO of 6.53%), mp 75°-80° C. (melts with gas evolution).

Quellen und Nachweise

ORD-Eintrag
ord-154fd7f99743497f9376353c58da2260
Quelldatensatz
uspto-grants-1987_01
Patentnummer
US04634551

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