HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxetane → 3-(4-Propyl-heptyl)-4-(3-hydroxypropyl)morpholine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxetane | HCID 10423 | — |
| Edukt | 3-(4-Propylheptyl)morpholine | HCID 11096343 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-(4-Propyl-heptyl)-4-(3-hydroxypropyl)morpholine | HCID 19870277 | 86,2% |
Reaktionsschritte
A mixture of 22.7 grams (0.1 mole) of 3-(4-propyl-heptyl)morpholine, 6.4 grams (0.11 moles) trimethyleneoxide and 150 ml. 96% ethanol was kept at 150°-200° C. for 15 hours in an autoclave. Distillation of the reaction mixture gave 24.6 g (86%) of 3-(4-propyl-heptyl)-4-(3-hydroxypropyl)morpholine), boiling point 122°-124° C./0.01 mm Hg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04636382 |
| Quelldatensatz | uspto-grants-1987_01 |
| ORD ID | ord-fad4245dbc354722ba3c23de7711c6c4 |
| Quellennotiz | uspto-grants-1987_01 |