HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → N-[2-(benzo[b]thien-3-yl)ethyl]adenosine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | Benzo[b]thiophene-3-ethanamine | HCID 26743 | — |
| Edukt | 6-Chloropurine riboside | HCID 93003 | — |
| Produkt | N-[2-(benzo[b]thien-3-yl)ethyl]adenosine | HCID 13686648 | — |
Reaktionsschritte
The title compound was prepared as in Example 1 using 6-chloropurine riboside (1.15 g, 4 mmol), 2-(3-benzo[b]thienyl)ethylamine.HCl (CAS Number 148585-66-1) (1.0 g, 4.6 mmol), and triethylamine (1.1 g, 11 mmol); yield 1.5 g (88%), mp 173°-174° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04636493 |
| Quelldatensatz | uspto-grants-1987_01 |
| ORD ID | ord-9d2e18fdd103489087644af369a02906 |
| Quellennotiz | uspto-grants-1987_01 |