Thionyl Chloride → HCID 178444488, Verbindung

HRID 980424

Reaktionsgleichung

Reaktionsgleichung von HRID 980424
[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([CH2:12][C:13]([OH:15])=O)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5].S(Cl)([Cl:18])=O>>[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([CH2:12][C:13]([Cl:18])=[O:15])[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 178444491HCID 178444491, Verbindung

Produkt 1

HCID 178444488HCID 178444488, Verbindung

Versuchsvorschrift

For conversion into the acid chloride, trans-4-pentylcyclohexylacetic acid (12.0 g, 0.0566 mol) was reacted for about 1 hour on an oil bath at 80° C. with thionyl chloride (50 ml). The solution obtained was evaporated under reduced pressure, treated with absolute toluene (50 ml) and once more evaporated under reduced pressure.

Aufarbeitung

  1. customThe solution obtained
  2. customwas evaporated under reduced pressure
  3. additiontreated with absolute toluene (50 ml)
  4. customonce more evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-f5c682759cb14903a7140f0f7b826a0a
Quelldatensatz
uspto-grants-1987_01
Patentnummer
US04637897

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